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SUPEREX F-500

Supercritical Extraction System

F-500
  • CO₂ is used as the primary solvent
  • 500 mL extraction vessel operating at up to 345 bar and 70°C
  • 50 mL Falcon tube
  • High-pressure mechanical filtration system
  • PLC-based automation system
  • 7” touchscreen control interface
  • Integrated chiller cooling unit
  • Pneumatically driven booster-type CO₂ pump
  • System can automatically reach the set pressure and set temperature values
  • Adjustable dynamic and static operation times
  • Sample collection using standard laboratory-grade Falcon tubes
  • Mechanical flowmeter for visual monitoring of CO₂ flow
  • Safety relief valve on the high-pressure reactor

Ürün Açıklaması

The F-500 with 500 ml extractor column offers compact design and stands out with easy sample loading, unloading, and cleaning features. It performs extraction in continuous dynamic CO2 flow mode with parameters adjustable from a touchscreen interface. Extracts directly into Falcon tubes with secondary Falcon separator liquid trapping feature.

Technical Specifications

Extraction vessel(s)
Number of vessels 1
Working volume of one vessel 0.5 L
Maximum operating temperature +70 °C, optionally up to 200 °C
Maximum operating pressure 345 bar (optionally up to 700 bar)
Test pressure 580 bar
Material Stainless steel (AISI 316L)
Separators for fractionation
Number of separators 2 (optionally 3)
Working volume of one separator 150 mL
Maximum operating temperature +70 °C
Maximum operating pressure SP-1 = 200 bar (adjustable), SP-2 = 100 bar
Test pressure 350 bar (or 160 bar for a working pressure of 100 bar)
Material Stainless steel (AISI 316L)
High pressure pump
Maximum CO2 mass flow rate 50 g/min at MAWP
Pump type Dual-stage piston gas booster with steel (CK-45) housing and pneumatic drive (for up to 345 bar), or a hydraulic pump with fluid reservoir (for pressures higher than 345 bar).
Heating block
Electric resistance heater 0.8 kW (or 4.5 kW for a maximum temperature of 200 °C)
Cooling unit (chiller)
Recirculating chiller, cooling power 1000 kcal/hr
Type of heat exchanger Tubular
Power requirements
Supply 220 V, single phase (6 kW)
Energy and CO2 consumption
Average power usage 4 kWh
Average CO2 usage ≤75 g per extraction cycle (CO2 recovery efficiency 90–95%)
Automatic back pressure regulators (aBPR)

The CO2 flow rate is precisely controlled by automatic back pressure regulators, reducing potential for operator error. Mass flow rate is monitored by installing the optional Coriolis mass flow meter.

Industrial automation system
PLC The system control panel is used to set and monitor all process conditions of pressure, temperature, solvent and co-solvent supply, pressure reduction and CO2 recycling. The software fully automates the extraction process (including static and dynamic extraction modes) and includes exhaustive routines for emergency shutdown.
Saving process parameters Up to 50 sets of process parameters may be saved into the system memory for rapid reloading.
Co-solvent system
Maximum co-solvent flow rate 30 ± 5 mL/min
Pump type Booster with a maximum working pressure of 360 bar (optionally 720 bar)
Disruption of raw material cells and cell walls via rapid pressure drop

Time-programmable sudden pressure drop during extraction facilitates expansion of CO2 that has penetrated the cells of the raw material. This rapid expansion ruptures cell walls and increases both the recovery of extract as well as the extraction rate.

Technical safety

Potential hazards caused by dangerous increases in pressure, temperature, and/or wear of sealing elements are completely prevented by software using a system of instrumentation and safety valves installed on each high-pressure element. In case of danger, the installation goes into emergency mode and all systems can be turned off using the emergency shutdown button.

Certifications

The system is fully certified under Directive 2006/42/EC and possesses the Conformité Européenne (CE) marking.

Optional Modules & Upgrades
CO2 liquefaction unit (chiller)
Co-solvent pump (30 mL/min)
Pressure increase to 700 bar
Impregnation module
Micronization module
Coriolis flowmeter, Bass Instruments
Maintenance Package (5 years)
Switch to AISI 304 stainless steel
Installation & Layout

Compact benchtop laboratory footprint. Installation and training of equipment operators (1 main operator and 1 supporting personnel) may take place at the production site or other location.

Product Comparison Table

Product
Volume

Pressure

Temperature

Separator

CO₂ Flow
SC-500 0.5 L 345 bar +70 °C 2 50 g/min
F-500
This Product
0.5 L 345 bar +70 °C 2 50 g/min
SC-1000 1 L 345 bar +70 °C 2 100 g/min
SUPEREX SC-1000 SUB-CRITICAL 1 L 345 bar +70 °C 2 100 g/min
TH-1000 1 L 345 bar +70 °C 2 100 g/min
F-1000 1 L 345 bar +70 °C 2 100 g/min
SC-2000 2 L 345 bar +70 °C 2 200 g/min
SC-4000 4 L 345 bar +70 °C 2 400 g/min
AERO-1000 1.0 L 345 bar +70 °C 2 100 mL/min
AERO-5000 5 L 345 bar +70 °C 2 500 mL/min